Kleiböhmer Environmental Analysis

1. Auflage 2001
ISBN: 978-0-08-050576-3
Verlag: Elsevier Science & Techn.
Format: PDF
Kopierschutz: 1 - PDF Watermark

E-Book, Englisch, 342 Seiten, Web PDF

'Environmental Analysis' covers a compilation of analytical methods for the determination of a wide range of environmental priority pollutants, including amines, polycyclic aromatic hydrocarbons, pesticides, phenols, PCBs, and also including organometallic species, polycyclic aromatic sulphur heterocycles and metabolites of polycyclic aromatic hydrocarbons. For all environmental pollutants, an overview and an assessment of value of a broad range of relevant methods including conventional techniques but also of advanced separation and sample preparation techniques given, with all possible matrices being considered.
This book does not only give up-to-date material on sampling and sample pre-treatment, extraction techniques, clean-up, pre-fractionation, different types of chromatographic methods and quality assurance, but also information on actual and upcoming analytical problems, such as the determination of polycyclic aromatic sulphur heterocycles and of metabolites of PAH. The final chapter is devoted to the important role of analytic separation methods in water quality control.
Experienced and well-known authors have contributed their knowledge and expertise to individual chapters.

Autoren/Hrsg.

Kleiböhmer, W.

Inhaltsverzeichnis

1;Cover;1
2;Contents;10
3;Editor’s Preface;6
4;Series Editor’s Preface;8
5;List of Contributors;18
6;Chapter 1. Gas chromatographic analysis of environmental amines with selective detectors;20
6.1;1.1 Introduction;20
6.2;1.2 Selective detectors for gas chromatography of amines;26
6.3;1.3 Applications in environmental amine analysis;36
6.4;1.4 Conclusions;48
6.5;1.5 References;50
7;Chapter 2. Modern techniques for the analysis of polycyclic aromatic hydrocarbons;58
7.1;2.1 Introduction;58
7.2;2.2 Development of instrumental techniques for PAH analysis;59
7.3;2.3 Sample preparation and extraction ;77
7.4;2.4 Concluding remarks;88
7.5;2.5 References;88
8;Chapter 3. Separation methods in the analysis of polycyclic aromatic sulfur heterocycles;94
8.1;3.1 Introduction;94
8.2;3.2 Sample workup for PASH analysis;98
8.3;3.3 Class separation of PAHs and PASHs ;99
8.4;3.4 Liquid chromatographic properties of PASHs;107
8.5;3.5 Gas chromatographic properties of PASHs;107
8.6;3.6 Heteroatom-substituted PASHs;112
8.7;3.7 Compounds with one other heterocyclic ring;113
8.8;3.8 PASHs in reference materials;114
8.9;3.9 Commercial sources of PASHs;115
8.10;3.10 References;115
9;Chapter 4. Polycyclic aromatic hydrocarbon (PAH) metabolites;118
9.1;4.1 Introduction;118
9.2;4.2 Metabolism;119
9.3;4.3 Biological monitoring;121
9.4;4.4 References;136
10;Chapter 5. Pesticides defined by matrix;142
10.1;5.1 Introduction;142
10.2;5.2 Extraction from water;143
10.3;5.3 Liquid–liquid extraction;146
10.4;5.4 Solid phase extraction;150
10.5;5.5 Solid phase microextraction;162
10.6;5.6 Extraction from soil;167
10.7;5.7 Microwave-assisted extraction;172
10.8;5.8 Accelerated solvent extraction;176
10.9;5.9 Supercritical fluid extraction ;180
10.10;5.10 Other solid/liquid techniques;188
10.11;5.11 Future prospects;190
10.12;5.12 Recommended further reading;190
10.13;5.13 References;191
11;Chapter 6. Phenols;194
11.1;6.1 Introduction;194
11.2;6.2 Extraction and preconcentration techniques;197
11.3;6.3 Chromatographic analysis;216
11.4;6.4 Capillary electrophoresis;242
11.5;6.5 Immunochemical methods;249
11.6;6.6 Conclusions;249
11.7;6.7 References;250
12;Chapter 7. Polychlorinated biphenyls;256
12.1;7.1 Introduction;256
12.2;7.2 Sampling and sample-pretreatment;258
12.3;7.3 Extraction;259
12.4;7.4 Clean-up;261
12.5;7.5 Pre-fractionation;263
12.6;7.6 GC analysis;267
12.7;7.7 Quality assurance;278
12.8;7.8 References;279
13;Chapter 8. Metal Species;282
13.1;8.1 Introduction to metal species;282
13.2;8.2 The meaning of ‘speciation’;282
13.3;8.3 Speciation of elements;282
13.4;8.4 Dynamics of species ;285
13.5;8.5 Errors during pre-treatment of samples for species determination;286
13.6;8.6 Analytical tools for species determination;289
13.7;8.7 Future aspects;290
13.8;8.8 Outlook;293
13.9;8.9 References;293
14;Chapter 9. Water Quality;296
14.1;9.1 Introduction;296
14.2;9.2 Definitions;299
14.3;9.3 Policy and legislative regulations;300
14.4;9.4 The current situation;307
14.5;9.5 Parameters to assess water quality;317
14.6;9.6 Sum parameters vs. single substance analysis;322
14.7;9.7 Sampling and sampling strategies;326
14.8;9.8 New sample preparation methods for organic micropollutants;329
14.9;9.9 New analytical methods for organic pollutants;331
14.10;9.10 References;333
15;Subject Index;338