Misra | Spectroscopy and Characterization of Nanomaterials and Novel Materials | Buch | 978-3-527-34937-1 | sack.de

Buch, Englisch, 528 Seiten, Format (B × H): 170 mm x 244 mm, Gewicht: 1134 g

Misra

Spectroscopy and Characterization of Nanomaterials and Novel Materials

Experiments, Modeling, Simulations, and Applications
1. Auflage 2022
ISBN: 978-3-527-34937-1
Verlag: WILEY-VCH

Experiments, Modeling, Simulations, and Applications

Buch, Englisch, 528 Seiten, Format (B × H): 170 mm x 244 mm, Gewicht: 1134 g

ISBN: 978-3-527-34937-1
Verlag: WILEY-VCH


Spectroscopy and Characterization of Nanomaterials and Novel Materials
Comprehensive overview of nanomaterial characterization methods and applications from leading researchers in the field
In Spectroscopy and Characterization of Nanomaterials and Novel Materials: Experiments, Modeling, Simulations, and Applications, the editor Prabhakar Misra and a team of renowned contributors deliver a practical and up-to-date exploration of the characterization and applications of nanomaterials and other novel materials, including quantum materials and metal clusters. The contributions cover spectroscopic characterization methods for obtaining accurate information on optical, electronic, magnetic, and transport properties of nanomaterials.
The book reviews nanomaterial characterization methods with proven relevance to academic and industry research and development teams, and modern methods for the computation of nanomaterials’ structure and properties - including machine-learning approaches - are also explored. Readers will also find descriptions of nanomaterial applications in energy research, optoelectronics, and space science, as well as: - A thorough introduction to spectroscopy and characterization of graphitic nanomaterials and metal oxides
- Comprehensive explorations of simulations of gas separation by adsorption and recent advances in Weyl semimetals and axion insulators
- Practical discussions of the chemical functionalization of carbon nanotubes and applications to sensors
- In-depth examinations of micro-Raman imaging of planetary analogs

Perfect for physicists, materials scientists, analytical chemists, organic and polymer chemists, and electrical engineers, Spectroscopy and Characterization of Nanomaterials and Novel Materials: Experiments, Modeling, Simulations, and Applications will also earn a place in the libraries of sensor developers and computational physicists and modelers.

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Preface  xix

About the Editor  xxvii

 

Part I Spectroscopy and Characterization 1

 

1 Spectroscopic Characterization of Graphitic Nanomaterials and Metal Oxides for Gas Sensing 3

Olasunbo Farinre, Hawazin Alghamdi, and Prabhakar Misra

1.1 Introduction and Overview  3

1.1.1 Graphitic Nanomaterials  3

1.1.1.1 Synthesis of Graphitic Nanomaterials  5

1.1.2 Metal Oxides  8

1.2 Spectroscopic Characterization of Graphitic Nanomaterials and Metal Oxides 9

1.2.1 Graphitic Nanomaterials  9

1.2.1.1 Characterization of Carbon Nanotubes (CNTs)  10

1.2.1.2 Characterization of Graphene and Graphene Nanoplatelets (GnPs)  11

1.2.2 Characterization of Tin Dioxide (SnO2)  12

1.3 Graphitic Nanomaterials and Metal Oxide-Based Gas Sensors  19

1.3.1 Fabrication of Graphitic Nanomaterials-Based Gas Sensors  19

1.3.1.1 Carbon Nanotube (CNT)-Based Gas Sensors  19

1.3.1.2 Graphene and Graphene Nanoplatelet (GnP)-Based Gas Sensors  20

1.3.2 Fabrication of Metal Oxide-Based Gas Sensors  21

1.3.2.1 Tin Dioxide (SnO2)-Based Gas Sensors  23

1.4 Conclusions and Future Work 24 Acknowledgments 26 References 26

 

2 Low-dimensional Carbon Nanomaterials: Synthesis, Properties, and Applications Related to Heat Transfer, Energy Harvesting, and Energy Storage 33

Mahesh Vaka, Tejaswini Rama Bangalore Ramakrishna, Khalid Mohammad, and Rashmi Walvekar

2.1 Introduction  33

2.2 Synthesis and Properties of Low-dimensional Carbon Nanomaterials  35

2.2.1 Zero-dimensional Carbon Nanomaterials (0-DCNs)  35

2.2.1.1 Fullerene  35

2.2.1.2 Carbon-encapsulated Metal Nanoparticles  35

2.2.1.3 Nanodiamond  37

2.2.2 Onion-like Carbons  38

2.2.3 One-dimensional Carbon Nanomaterials  39

2.2.3.1 Carbon Nanotube  39

2.2.3.2 Carbon Fibers  39

2.2.4 Two-dimensional Carbon Nanomaterials  40

2.3 Applications  42

2.3.1 Hydrogen Storage  42

2.3.2 Solar Cells  43

2.3.3 Thermal Energy Storage  44

2.3.4 Energy Conversion  45

2.4 Conclusions  46

References  46

 

3 Mesoscale Spin Glass Dynamics  55

Samaresh Guchhait

3.1 Introduction  55

3.2 What Is a Spin Glass?  56

3.2.1 Spin Glass and Its Correlation Length  57

3.2.2 Mesoscale Spin Glass Dynamics  60

3.3 Summary 64 Acknowledgments 64 References 64

 

4 Raman Spectroscopy Characterization of Mechanical and Structural Properties of Epitaxial Graphene 67

Amira Ben Gouider Trabelsi, Feodor V. Kusmartsev, Anna Kusmartseva, and Fatemah Homoud Alkallas

4.1 Introduction  67

4.2 Epitaxial Graphene Mechanical Properties Investigation  68

4.2.1 Optical Location of Epitaxial Graphene Layers  68

4.2.2 Raman Location of Mechanical Properties Changes  71

4.2.2.1 Graphene 2D Mode  71

4.2.2.2 G Mode Investigation  74

4.2.2.3 Strain Percentage  76

 4.3 Raman Polarization Study  77

4.3.1 Size Domain of Graphene Layer  77

4.3.2 Polarization Study  78

4.4 Conclusions 80 Acknowledgments 80 References 80

 

5 Raman Spectroscopy Studies of III–V Type II Superlattices  83

Henan Liu and Yong Zhang

5.1 Introduction  83

5.2 Raman Study on InAs/GaSb SL  84

5.2.1 Analysis on (001) Scattering Geometry  85

5.2.2 Analysis on (110) Scattering Geometry  86

5.3 Raman Study on InAs/InAs1-xSbx SL  90

5.3.1 Raman Results for the Constituent Bulks and InAs1-xSbx Alloys  90

5.3.2 Analysis on (001) Scattering Geometry for the SLs  93

5.3.3 Analysis on (110) Scattering for the SLs  95

5.4 A Comparison Among the InAs/InAs1-xSbx, InAs/GaSb, and GaAs/AlAs SLs 97

5.5 Conclusion  98

References  98

 

6 Dissecting the Molecular Properties of Nanoscale Materials Using Nuclear Magnetic Resonance Spectroscopy 101

Nipanshu Agarwal and Krishna Mohan Poluri

6.1 Introduction to Nanomaterials  101

6.2 Techniques Used for Characterization of Nanomaterials  104

6.3 Nuclear Magnetic Resonance (NMR) Spectroscopy  105

6.3.1 Principle of NMR Spectroscopy  106

6.3.2 Various NMR Techniques Used in Nanomaterial Characterization  106

6.3.2.1 One-dimensional NMR Spectroscopy  108

6.3.2.2 Relaxometry (T1 and T2)  108

6.3.2.3 Two-dimensional NMR Spectroscopy  110

6.3.3 Advantages and Disadvantages of Using NMR Spectroscopy  114

6.4 Applications of NMR in Nanotechnology  115

6.4.1 NMR for Characterization of Nanomaterials  115

6.4.1.1 Characterization of Gold Nanomaterials by NMR  115

6.4.1.2 Characterization of Organic Nanomaterials by NMR  119

6.4.1.3 Characterization of Quantum Dots and Nanodiamonds by NMR 120

6.4.2 Elucidating the Molecular Characteristics/Interactions of Nanomaterials Using NMR 120

6.4.2.1 Characterizing Nanodisks Using Paramagnetic NMR  120

6.4.2.2 Characterizing Nanomaterials Using Low Field NMR (LF-NMR) 123

6.4.2.3 Analyzing Nanomaterial Interactions Using 2D NMR Techniques  123

6.4.3 Characterization of Magnetic Contrast Agents (MR-CAs)  128

6.5 Conclusions 132 Acknowledgments 132 References 132

 

7 Charge Dynamical Properties of Photoresponsive and Novel Semiconductors Using Time-Resolved Millimeter-Wave Apparatus 149

Biswadev Roy, Branislav Vlahovic, M.H. Wu, and C.R. Jones

7.1 Introduction  149

7.1.1 Why Charge Dynamics for Novel Materials in the Millimeter-Wave Regime? 150

7.1.2 Underlying Theory of Operation and Time-Resolved Data: Treatment of Internal Fields in Samples 154

7.1.3 Apparatus Design and Instrumentation  156

7.1.4 Sensitivity Analysis and Dynamic Range  158

7.1.5 Calibration Factor  159

7.2 Stud


Prabhakar Misra, PhD, is a Professor in the Department of Physics and Astronomy at Howard University in Washington, DC. He has over 30 years of experience researching the detection and spectroscopic characterization of jet-cooled free radicals, ions and stable molecules of relevance to combustion phenomena and plasmas, Raman spectroscopy and Molecular Dynamics simulation of nanomaterials for gas-sensing applications, and other contemporary areas in experimental atomic and molecular physics and condensed matter physics.



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