Mitra Sample Preparation Techniques in Analytical Chemistry


1. Auflage 2004
ISBN: 978-0-471-45782-4
Verlag: John Wiley & Sons
Format: PDF
Kopierschutz: Adobe DRM (»Systemvoraussetzungen)

E-Book, Englisch, 488 Seiten, E-Book

Reihe: Chemical Analysis: A Series of Monographs on Analytical Chemistry and Its Applications

ISBN: 978-0-471-45782-4
Verlag: John Wiley & Sons
Format: PDF
Kopierschutz: Adobe DRM (»Systemvoraussetzungen)



The importance of accurate sample preparation techniques cannot beoverstated--meticulous sample preparation is essential. Oftenoverlooked, it is the midway point where the analytes from thesample matrix are transformed so they are suitable for analysis.Even the best analytical techniques cannot rectify problemsgenerated by sloppy sample pretreatment.
Devoted entirely to teaching and reinforcing these necessarypretreatment steps, Sample Preparation Techniques in AnalyticalChemistry addresses diverse aspects of this important measurementstep. These include:
* State-of-the-art extraction techniques for organic and inorganicanalytes
* Sample preparation in biological measurements
* Sample pretreatment in microscopy
* Surface enhancement as a sample preparation tool in Raman and IRspectroscopy
* Sample concentration and clean-up methods
* Quality control steps
Designed to serve as a text in an undergraduate or graduate levelcurriculum, Sample Preparation Techniques in Analytical Chemistryalso provides an invaluable reference tool for analytical chemistsin the chemical, biological, pharmaceutical, environmental, andmaterials sciences.

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Autoren/Hrsg.


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Contributors.
Preface.
Chapter 1. Sample Preparation: An Analytical Perspective(Somenath Mitra and Roman Brukh).
SECTION A: EXTRACTION AND ENRICHMENT IN SAMPLE PREPARATION.
Chapter 2. Principles of Extraction and the Extraction ofSemivolatile Organics From Liquids (MarthaJ.M. Wells).
Chapter 3. Extraction of Semivolatile Organic Compounds FromSolid Matrices (Dawen Kou and Somenath Mitra).
Chapter 4. Extraction of Volatile Organic Compounds From Solidsand Liquids (Gregory C. Slack, et al.).
Chapter 5. Preparation of Samples for Metals Analysis (BarbaraB. Kebbekus).
SECTION B: SAMPLE PREPARATION FOR NUCLEIC ACIDANALYSIS.
Chapter 6. Sample Preparation in DNA Analysis (SatishParimoo and Bhama Parimmo).
Chapter 7. Sample Preparation in RNA Analysis (BhamaParimoo and Satish Parimoo).
Chapter 8. Techniques for the Extraction, Isolation andPurification of Nucleic Acids (Mahesh Karwa and SomenathMitra).
SECTION C: SAMPLE PREPARATION IN MICROSCOPY ANDSPECTROSCOPY.
Chapter 9. Sample Preparation for Microscope and SpectroscopicCharacterization of Solid Surfaces and Films (SharmilaM. Mukhopadhyay).
Chapter 10. Surface Enhancement by Sample and SubstratePreparation Techniques in Raman and Infrared Spectroscopy (ZafarIqbal).
Index.


SOMENATH MITRA. PHD, is Professor of Chemistry and Environmental Science at the New Jersey Institute of Technology. He is coauthor of the textbook Environmental Chemical Analysis. In addition, he has published extensively in peer-reviewed journals of chemistry and analytical sciences.



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