NMR - From Spectra to Structures

An Experimental Approach
2. revidierteand exp.Auflage 2007
ISBN: 978-3-540-72195-6
Verlag: Springer Berlin Heidelberg

Buch, Englisch, 207 Seiten, Paperback, Format (B × H): 155 mm x 235 mm, Gewicht: 347 g

Nuclear magnetic resonance spectroscopy is one of the most powerful analytical methods. This practice-oriented textbook aims at teaching how NMR experiments should be used to make structural asssignments. The book is intended as a practical guide for students and laboratory personnel, so that the emphasis is on practical rather than on theoretical aspects, which are treated only to the extent necessary to understand the experiments and to interpret the results.
The second edition has been expanded to include several other heteronuclei (N, F, Si, Se, Cd, Sn/Sn, Pt, Pb) and a new chapter on solid state NMR. The problems section has been enlarged and now includes 50 problems. These are of different degrees of complexity and in all cases include two-dimensional (2D) methods as well as standard proton and carbon 1D spectra.

Zielgruppe

Graduate

Autoren/Hrsg.

Costisella, Burkhard

Mitchell, Terence N.

Fachgebiete

• Naturwissenschaften Physik Physik Allgemein Experimentalphysik
• Naturwissenschaften Chemie Organische Chemie
• Naturwissenschaften Chemie Analytische Chemie Massenspektrometrie, Spektroskopie, Spektrochemie

Inhaltsverzeichnis

NMR Experiments.- 1D Experiments.- 2D Experiments.- Quadrupolar Nucleus Experiments.- HPLC-NMR Coupling.- Other Spin-1/2 Nuclei.- Solid State NMR.- Worked Example and Problems.- Section 1.- Worked Example.- Problems.- Section 2.

Über Autor(innen)

Introduction

Part I - NMR Experiments

1. 1D Experiments

2. 2D Experiments

3. Quadrupolar Nucleus Experiments

4. HPLC-NMR Coupling

Appendix: Reference List

Part II - Worked Example and Problems

Introduction

Worked Example

Problems

Index