Mitchell / Costisella NMR - From Spectra to Structures

An Experimental Approach
2. revidierteand exp.Auflage 2007
ISBN: 978-3-540-72196-3
Verlag: Springer
Format: PDF
Kopierschutz: 1 - PDF Watermark

E-Book, Englisch, 222 Seiten, eBook

Nuclear magnetic resonance spectroscopy is one of the most powerful analytical methods. This practice-oriented textbook aims at teaching how NMR experiments should be used to make structural asssignments. The book is intended as a practical guide for students and laboratory personnel, so that the emphasis is on practical rather than on theoretical aspects, which are treated only to the extent necessary to understand the experiments and to interpret the results. The second edition has been expanded to include several other heteronuclei ( 15 N, 19 F, 29 Si, 77 Se, 113 Cd, 117 Sn/ 119 Sn, 195 Pt, 207 Pb) and a new chapter on solid state NMR. The problems section has been enlarged and now includes 50 problems. These are of different degrees of complexity and in all cases include two-dimensional (2D) methods as well as standard proton and carbon 1D spectra.

Zielgruppe

Graduate

Autoren/Hrsg.

Mitchell, Terence N.

Costisella, Burkhard

Inhaltsverzeichnis

NMR Experiments.- 1D Experiments.- 2D Experiments.- Quadrupolar Nucleus Experiments.- HPLC-NMR Coupling.- Other Spin-1/2 Nuclei.- Solid State NMR.- Worked Example and Problems.- Section 1.- Worked Example.- Problems.- Section 2.

Über Autor(innen)

IntroductionPart I - NMR Experiments1. 1D Experiments2. 2D Experiments3. Quadrupolar Nucleus Experiments4. HPLC-NMR CouplingAppendix: Reference List Part II - Worked Example and ProblemsIntroductionWorked ExampleProblemsIndex